PRODUCTS & SERVICES : HEAT TREATMENT COURSE : Course description and syllabus

Course description. Learn the heat treatment of ruby-sapphire from Ted Themelis, one of the world's foremost authority in the subject matter. You will gain invaluable insights into the unique world of the gem treatments. And more importantly, will be prepared to take your place among the leading figures in the gem & jewelry industry. Ted's training course is the only one of its kind available today in the world that provides unique training in the heat treatment of ruby-sapphire.

What you will learn: For a week you will study under the personal tutelage and watchful eyes of Ted working together on actual lab environment. One-to-one instruction supplemented by powerful presentations and hands-on practical experience, all of which ultimately will empower you with confidence to walk out at the end of the course and find yourself enriched with knowledge and skills to put you miles ahead of your competition. Although, at the end of the course you will not become an expert in heating ruby-sapphire, this course will help you to develop a comprehensive knowledge in your career that ultimately help your business.

Who will benefit:

  • Gemologists and instructors of gemology, students and other individuals wishing to acquire knowledge and skills in high-temperature furnace technology and in the heat-treating ruby & sapphire.
  • Next generation research-gemologists focusing on forensic gemology, beyond the ordinary.
  • Gemstone miners, producers, importers, distributors and dealers who need to understand the heat treatment technology to help them evaluate the potentiality of their gem inventory.
  • Gemstone treaters wishing to expand their current skills and knowledge and to improve their methodology in heat-treating ruby & sapphire.
  • Individuals wishing to acquire the technical skills to develop their own gem treatment facilities

Syllabus:

The course features a) theory-demonstrations and b) on-hands practical experience. Theoretical knowledge convey the principals, definitions and fundamentals in heat-treating technology. On-hands practical experience allows preparation of samples and subsequent heating on a high-temperature top loading muffle furnace.

Part I. (Powerpoint presentations and demonstrations)

  • Review the historical aspects in heating ruby-sapphire
  • Understand corundum as an imperfect crystal
  • Recognize the various treatment types of ruby-sapphire
  • Plan the strategy in heating ruby-sapphire
  • Gain knowledge in heat and the effect of heat in ruby-sapphire
  • Comprehend temperature measurement (types, description, calibration)
  • Get the fundamentals and concept of oxidizing-reducing atmosphere, buffering & non-buffering reactions, gas fugacity, and influence of gas fugacity in heating ruby & sapphire
  • Master the muffle concept and how to obtain precise gas mixtures
  • Understand gas technology and gas mixing
  • Learn the concept of diffusion phenomenology and its role in heating ruby-sapphire
  • Learn about additives and fluxes: methodology, application, safety & handling. Learn how to prepare and apply flux-melt additives and reagent-grade powers for heating ruby-sapphire.
  • Develop the skills in understanding the heat-treatment processes of ruby, pink, "padparadscha", orange, yellow, purple/violet, sapphire, yellow, blue, blue/green, green and star sapphire.
  • Become skilled in setting up the heat-treatment parameters in heating ruby-sapphire. Learn how to prepare and run a heating process.
  • Be familiar and work with different types of ceramics used for heating ruby-sapphire.
  • Learn about and examine the anatomy of open-flame furnaces used in heating ruby-sapphire, i.e. traditional kilns (coke, lignite), diesel-oxy furnaces, LPG-OXY, etc.
  • Watch a very rare documentary videotape in heating geuda sapphires using a traditional LPG-oxy furnace filmed by Ted in 1985.
  • Understand the various types of electric furnaces used in heating ruby-sapphire (box, muffle, graphite, induction, vacuum, high-pressure, etc.)
  • Learn the "dry" and "wet' beryllium heating processes of ruby-sapphire (methodology and processes of different types of corundum, inclusion features, handling-safety, stability, disclosure)
  • Comprehend the LIBS method in detecting beryllium in beryllium-treated ruby-sapphire
  • Learn the latest treatment of the lead-filled rubies, pink sapphires and examine different types of rubies before/after the treatment.
  • Be informed on the related technology of the re-crystallization process of blue sapphires and the heating procedures involved.
  • Recognize the integrity of the heat-treated ruby-sapphire and maintain consumer confidence with proper detection and disclosure.
  • Find out how to calculate cost effectiveness ratio and yields before/after the heating process.

Part II (Practical, hands-on workshop)

  • HEAT PROCESS #1. Select rubies and pink sapphires from Vietnam, Madagascar, Tanzania, etc. Prepare and execute a heating process using gas fugacity with/without fluxes.
  • HEAT PROCESS #2: Select, rubies & sapphires from Songea, Madagascar, Tunduru, etc. Prepare and execute a "dry" beryllium heating process using the electric furnace.
  • HEAT PROCESS #3: Demonstration of the most sought heating processes of blue sapphire as performed in Sri-Lanka and elsewhere using the LAKMINI furnace.

RESTRICTION: Due to the sensitive nature of the topics, taking photos or videotape recordings is strictly PROHIBITED.


JC Ephraim (July 2003 Class) mixing
additives used in the heating process.


Discussing the procedures to be taken in heating various types of sapphires. (Class April 2003)


Removing the crucible from the furnace after
the heating process.

An electric resistance 1800oC top-loaded, vertical muffle furnace fabricated by three students of class April 2003, based on Ted's tutelage. (Class April 2003)

 

 


Removing the gems from the crucibles after
the heat-treatment process(Class June 2004)


Demonstration of the "Lakmini" gas
combustion furnace (Class Dec. 2004)


Examining specimens after heat-treatment
process (Class May 2005)


Discussing heat-treated rubies after the process (Class May 2005)

Course materials:

  • A vertical muffle 1800oC electric furnace and a LAKMINI LPG-oxy will be available for demonstration (process #1, #2 and #3)
  • Selected rubies-sapphires, additives and ceramics needed for the practical process will be supplied. Suitable rubies-sapphires can be brought by the students for heating using heat-process #1, #2 or #3
  • Processing instruments, heating elements, ceramics, various furnace parts, fluxes and related materials are provided for demonstration purposes (not to be taken out of the class)
  • A gemological microscope assigned for each participant is provided throughout the course
  • A colored hard-copy of all presentations is supplied
  • REFERENCE books by Ted Themelis: "Heat-Treatment of Ruby & Sapphire", "Beryllium-Treated Rubies & Sapphires" and "Flux-Enhanced rubies & Sapphires" PLUS abstracts from the Gemlab Reports".

Gemlab 1800oC furnace
used in the training

Lakmini gas furnace used in the training session

Gemstones and ceramics provided for training

A microscope is assigned for each participant

Colored hard-copy of all presentations are provided

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